Silver mirrored bottles
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- Illumina-Mitglied
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Re: Silver mirrored bottles
You can make a potassium mirror by subliming the metal in an evacuated flask.
- andrewtretiakov
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Re: Silver mirrored bottles
Excellent! Is this done using hydrazine as a reducing agent? Please share your method. I've only done it using thermal decomposition of copper formate:
https://pubs.acs.org/doi/full/10.1021/ed101143r
Works pretty well but not as good as yours

Anyway, here is a photo Thanks,
A
- andrewtretiakov
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Re: Silver mirrored bottles
Thanks, I've been trying to do one but I have no access to a Schlenk line only a commercial standard vacuum pump.Glaskocher hat geschrieben: ↑Freitag 8. September 2023, 21:28You can make a potassium mirror by subliming the metal in an evacuated flask.
Still, I got this one a few years back: Not perfect but work in progress.
A
- mgritsch
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Re: Silver mirrored bottles
Formaldehyde works pretty well!andrewtretiakov hat geschrieben: ↑Sonntag 10. September 2023, 14:01Excellent! Is this done using hydrazine as a reducing agent? Please share your method.
I am still optimising the method a bit, but will post as soon as worked out properly.